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Structure tuning of metal phosphonates: Syntheses, structures and characterizations of two new lead (II) trisphosphonates
Tang, Si-Fu; Lv, Xiao-Xia; Li, Liang-Jun; Wang, Chao; Zhao, Xue-Bo
2014
发表期刊INORGANIC CHEMISTRY COMMUNICATIONS
卷号39页码:51-55
摘要Two lead (II) trisphosphonates, [Pb-3(H3L1)(2)(H2O)] (1) and [Pb-5(HL2)(H3L2)(H4L2)(H2O)(2)][(H2O)(2)] (2), have been synthesized from two trisphosphonate ligands and characterized by EA, IR, UV-vis, TGA, powder and single-crystal X-ray diffraction methods. The single-crystal X-ray diffraction analyses reveal that they both feature three-dimensional framework structures. The lead (II)ions are mainly five-coordinated, forming square pyramid coordination geometry. Although the two trisphosphonate ligands are very similar, different coordination modes and conformations are observed for them, suggesting that attachment of methyl groups to the central benzene ring has a major effect on the structure formation. They both absorb below 325 nm and are thermally robust. (C) 2013 Elsevier B.V. All rights reserved.
文章类型Article
关键词Phosphonates Lead Crystal Structure Characterization
WOS标题词Science & Technology ; Physical Sciences
DOI10.1016/j.inoche.2013.10.039
关键词[WOS]ORGANIC FRAMEWORKS ; CRYSTAL-STRUCTURES ; DIPHOSPHONATES ; LIGANDS ; TETRANUCLEAR ; LINKERS ; CLUSTER ; FILMS
收录类别SCI
语种英语
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
WOS记录号WOS:000330157700012
引用统计
文献类型期刊论文
条目标识符http://ir.qibebt.ac.cn/handle/337004/6227
专题储氢及新型纳孔材料团队(过去)
作者单位Chinese Acad Sci, Qingdao Inst Bioenergy & Bioproc Technol, Qingdao 266101, Peoples R China
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Tang, Si-Fu,Lv, Xiao-Xia,Li, Liang-Jun,et al. Structure tuning of metal phosphonates: Syntheses, structures and characterizations of two new lead (II) trisphosphonates[J]. INORGANIC CHEMISTRY COMMUNICATIONS,2014,39:51-55.
APA Tang, Si-Fu,Lv, Xiao-Xia,Li, Liang-Jun,Wang, Chao,&Zhao, Xue-Bo.(2014).Structure tuning of metal phosphonates: Syntheses, structures and characterizations of two new lead (II) trisphosphonates.INORGANIC CHEMISTRY COMMUNICATIONS,39,51-55.
MLA Tang, Si-Fu,et al."Structure tuning of metal phosphonates: Syntheses, structures and characterizations of two new lead (II) trisphosphonates".INORGANIC CHEMISTRY COMMUNICATIONS 39(2014):51-55.
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