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Acidic resin-catalyzed conversion of fructose into furan derivatives in low boiling point solvents
Hong Zhua; Quan Caoa; Chunhu Li; Xindong Mu
2011
发表期刊Accepted Manuscript
卷号11期号:1页码:0-16
摘要Conversion of fructose into furan derivatives 5-hydroxymethylfurfural (HMF) and 5-methoxymethylfurfural (MMF) is performed in tetrahydrofuran (THF) and methanol-organic solvent systems, catalysed by an acidic resin Amberlyst-15. The melted fructose can be converted into HMF on the surface of the solid resin catalyst in the presence of THF as an extracting phase, which is a good solvent for HMF and other by-products. The solid resin catalyst can be reused eleven times without losing its catalytic ability, with an average HMF yield of approximately 50%. Upon the addition of methanol, the generated HMF can further react with methanol to form MMF, and the total yield of HMF and MMF could be promoted to 65%. GC-MS analysis confirms the formation of a small amount of methyl levulinate in methanolorganic solvent system.
关键词Fructose 5-hydroxymethylfurfural 5-methoxymethylfurfural Methyl Levulinate Amberlyst-15
学科领域绿色化学催化
收录类别SCI
语种英语
文献类型期刊论文
条目标识符http://ir.qibebt.ac.cn/handle/337004/618
专题绿色化学催化研究组
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GB/T 7714
Hong Zhua,Quan Caoa,Chunhu Li,et al. Acidic resin-catalyzed conversion of fructose into furan derivatives in low boiling point solvents[J]. Accepted Manuscript,2011,11(1):0-16.
APA Hong Zhua,Quan Caoa,Chunhu Li,&Xindong Mu.(2011).Acidic resin-catalyzed conversion of fructose into furan derivatives in low boiling point solvents.Accepted Manuscript,11(1),0-16.
MLA Hong Zhua,et al."Acidic resin-catalyzed conversion of fructose into furan derivatives in low boiling point solvents".Accepted Manuscript 11.1(2011):0-16.
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