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Synthesis, Structures, and Properties of Two Novel Coordination Polymers with a V-shaped Diphosphonate Ligand
Lv, Xiaoxia1,2; Tang, Sifu1; Li, Liangjun1,2; Xu, Xianrui1,2; Zhao, Xuebo1
2013-08-01
发表期刊ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
卷号639期号:10页码:1845-1849
摘要

Two novel coordination polymers, [Cu(H2L)(bipy)(H2O)(2)]center dot H2O (1) and [Ni-2(H2L)(bipy)(2.5)(H2O)(6)]center dot(H2L)center dot 7H(2)O (2) with the V-shaped diphosphonate ligand (2,4,6-trimethyl-1,3-phenylene) bis(methylene) diphosphonic acid (H4L) were synthesized via hydrothermal reactions in the presence of auxiliary ligand 4,4'-bipyridine. Their structures were determined by single-crystal X-ray diffraction and further characterized by elemental analysis, infrared spectroscopy (IR), and thermogravimetric analysis (TGA). Compound 1 crystallizes in the Pnma space group and compound 2 crystallizes in the P2(1)2(1)2 space group. They display square-grid layer and bilayer two-dimensional network, respectively.

文章类型Article
关键词Diphosphonate Ligand V-shape Crystal Structure X-ray Diffraction Infrared Spectroscopy
WOS标题词Science & Technology ; Physical Sciences
DOI10.1002/zaac.201300185
关键词[WOS]METAL-ORGANIC FRAMEWORK ; TRINUCLEAR (NICUNIII)-CU-II-NI-II COMPLEXES ; ZEOLITIC IMIDAZOLATE FRAMEWORKS ; MAGNETIC-PROPERTIES ; CRYSTAL-STRUCTURE ; SMALL MOLECULES ; SEPARATION ; CHAIN ; CO2 ; CAPTURE
收录类别SCI
语种英语
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
WOS记录号WOS:000327704000024
引用统计
文献类型期刊论文
条目标识符http://ir.qibebt.ac.cn/handle/337004/6014
专题多相催化转化研究组
作者单位1.Chinese Acad Sci, Qingdao Inst Bioenergy & Bioproc Technol, Qingdao 266101, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
推荐引用方式
GB/T 7714
Lv, Xiaoxia,Tang, Sifu,Li, Liangjun,et al. Synthesis, Structures, and Properties of Two Novel Coordination Polymers with a V-shaped Diphosphonate Ligand[J]. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE,2013,639(10):1845-1849.
APA Lv, Xiaoxia,Tang, Sifu,Li, Liangjun,Xu, Xianrui,&Zhao, Xuebo.(2013).Synthesis, Structures, and Properties of Two Novel Coordination Polymers with a V-shaped Diphosphonate Ligand.ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE,639(10),1845-1849.
MLA Lv, Xiaoxia,et al."Synthesis, Structures, and Properties of Two Novel Coordination Polymers with a V-shaped Diphosphonate Ligand".ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE 639.10(2013):1845-1849.
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