QIBEBT-IR
Rapidly detecting tetrabromobisphenol A in soils and sediments by paper spray ionization mass spectrometry combined with isotopic internal standard
Liu, Huan1; Gao, Wei2,3; Tian, Yong1; Liu, Aifeng1; Wang, Zhenhua4; Cai, Yaqi5; Zhao, Zongshan1
2019
Source PublicationTALANTA
ISSN0039-9140
Volume191Pages:272-276
AbstractRapidly detecting trace levels of organic contaminants in complex mediums is a great challenge for mass spectrometry analysis. Especially in dealing with large quantities of soil samples, the laborious sample pretreatment process is exhausting and time consuming. Here, a simple method for quickly identifying and quantifying tetrabromobisphenol A (TBBPA) in soils and sediments has been developed via paper spray ambient mass spectrometry coupled with a stable isotope internal standard technique in this study. The soil and sediment extracts, spiked with a certain amount of C-13(12)-TBBPA (Ring-C-13(12)), are directly loaded and separated on chromatographic paper, sprayed and ionized by a high negative voltage, and ultimately analyzed by mass spectrometry without purification and chromatography separation processes. Data acquisition for each test can be finished within 1 min. In the quantification of TBBPA, a linear range of 0.1-100 mu g L-1, a limit of detection of 0.039 mu g L-1 and a relative standard deviation (c = 1.0 mu g L-1, n = 5) of 5.3% are obtained. The spiking recoveries range from 90.4% to 101.1% for analyzing ten soil and sediment samples (0.012-30.14 mu g g(-1) dw), suggesting that the method should be a promising strategy for rapidly detecting organic pollutants in soils and sediments.
KeywordPaper spray ionization mass spectrometry Tetrabromobisphenol A Soil Sediment
DOI10.1016/j.talanta.2018.08.069
WOS KeywordBROMINATED FLAME RETARDANTS ; ELECTROSPRAY-IONIZATION ; AMBIENT IONIZATION ; ANALYTICAL DEVICES ; BISPHENOL-A ; DERIVATIVES ; SAMPLES ; IDENTIFICATION ; DESORPTION ; QUANTIFICATION
Language英语
Funding ProjectNational Natural Science Foundation of China[21607161] ; National Natural Science Foundation of China[21537004] ; Scientific Instrument Developing Project of the Chinese Academy of Sciences[YZ201642] ; Primary Research & Development Plan of Shandong Province[2016GSF117039] ; State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences[KF2015-10]
WOS Research AreaChemistry
Funding OrganizationNational Natural Science Foundation of China ; Scientific Instrument Developing Project of the Chinese Academy of Sciences ; Primary Research & Development Plan of Shandong Province ; State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences
WOS SubjectChemistry, Analytical
WOS IDWOS:000447481600036
PublisherELSEVIER SCIENCE BV
Citation statistics
Cited Times:7[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.qibebt.ac.cn/handle/337004/11743
Collection中国科学院青岛生物能源与过程研究所
Corresponding AuthorTian, Yong; Zhao, Zongshan
Affiliation1.Chinese Acad Sci, Qingdao Inst Bioenergy & Bioproc Technol, CAS Key Lab Biobased Mat, Qingdao 266101, Peoples R China
2.Northeastern Univ, Coll Sci, Res Ctr Analyt Sci, Shenyang 110819, Liaoning, Peoples R China
3.Northeastern Univ, Coll Sci, Dept Chem, Shenyang 110819, Liaoning, Peoples R China
4.Shandong Acad Sci, Qilu Univ Technol, Shandong Anal & Tester Ctr, Jinan 250014, Shandong, Peoples R China
5.Chinese Acad Sci, Res Ctr Ecoenvironm Sci, State Key Lab Environm Chem & Ecotoxicol, Beijing 100085, Peoples R China
Recommended Citation
GB/T 7714
Liu, Huan,Gao, Wei,Tian, Yong,et al. Rapidly detecting tetrabromobisphenol A in soils and sediments by paper spray ionization mass spectrometry combined with isotopic internal standard[J]. TALANTA,2019,191:272-276.
APA Liu, Huan.,Gao, Wei.,Tian, Yong.,Liu, Aifeng.,Wang, Zhenhua.,...&Zhao, Zongshan.(2019).Rapidly detecting tetrabromobisphenol A in soils and sediments by paper spray ionization mass spectrometry combined with isotopic internal standard.TALANTA,191,272-276.
MLA Liu, Huan,et al."Rapidly detecting tetrabromobisphenol A in soils and sediments by paper spray ionization mass spectrometry combined with isotopic internal standard".TALANTA 191(2019):272-276.
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